Technology Process of C30H40BrN3O6
There total 4 articles about C30H40BrN3O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C27H34BrN3O6; allylmagnesium bromide;
In
tetrahydrofuran; diethyl ether;
at 0 ℃;
for 1.5h;
With
water; ammonium chloride;
In
tetrahydrofuran; diethyl ether;
for 0.166667h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.03 h / 180 °C / Microwave
2.1: lithium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 0.04 h / 170 °C / Microwave
2.2: 0.17 h
3.1: tetrahydrofuran; diethyl ether / 1.5 h / 0 °C
3.2: 0.17 h
With
1,8-diazabicyclo[5.4.0]undec-7-ene; lithium hexamethyldisilazane;
In
tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 20 °C
2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / N,N-dimethyl-formamide / 0.03 h / 180 °C / Microwave
3.1: lithium hexamethyldisilazane / tetrahydrofuran; N,N-dimethyl-formamide / 0.04 h / 170 °C / Microwave
3.2: 0.17 h
4.1: tetrahydrofuran; diethyl ether / 1.5 h / 0 °C
4.2: 0.17 h
With
carbon tetrabromide; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; diethyl ether; dichloromethane; N,N-dimethyl-formamide;
