Technology Process of C28H40N2O
There total 6 articles about C28H40N2O which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: potassium carbonate / N,N-dimethyl-formamide / 18 h / 20 °C
2.1: potassium carbonate / N,N-dimethyl-formamide / 6 h / 80 °C
3.1: palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 6 h / 90 °C
4.1: sodium hydroxide / ethanol / 3 h / Reflux
4.2: 2 h / 40 °C
4.3: 1 h / 20 °C
5.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C
6.1: palladium 10% on activated carbon; hydrogen / ethanol / 20 h / 20 °C / 750.08 Torr
With
lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen; palladium diacetate; potassium carbonate; tris-(o-tolyl)phosphine; sodium hydroxide;
In
tetrahydrofuran; ethanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.bmc.2013.05.035
- Guidance literature:
-
With
palladium 10% on activated carbon; hydrogen;
In
ethanol;
at 20 ℃;
for 20h;
under 750.075 Torr;
DOI:10.1016/j.bmc.2013.05.035
- Guidance literature:
-
Multi-step reaction with 2 steps
1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 20 °C
2: palladium 10% on activated carbon; hydrogen / ethanol / 20 h / 20 °C / 750.08 Torr
With
lithium aluminium tetrahydride; palladium 10% on activated carbon; hydrogen;
In
tetrahydrofuran; ethanol;
DOI:10.1016/j.bmc.2013.05.035
