1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine

Base Information

Chemical Name:1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine
CAS No.:113430-91-4
Molecular Formula:C₂₆H₃₉N₃O₁₂
Molecular Weight:585.609
Hs Code.:

Synonyms:1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine

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Chemical Property of 1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine

Chemical Property:

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Technology Process of 1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine

There total 4 articles about 1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 6290-05-7
Diethyl iminodiacetate

: 113430-90-3
1-(2-nitro-4,5-dimethoxyphenyl)ethane-1,2-diyl 1,2-dibromide

: 113430-91-4
1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine

Guidance literature:: for 504h; under 258574 Torr;
DOI:10.1021/jo00244a022

Reference yield:

: 65907-71-3
1,2-dimethoxy-4-nitro-5-vinylbenzene

: 113430-91-4
1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / Br₂ / CH₂Cl₂

2: 12 percent / Na₂CO₃ / acetonitrile / Heating

With bromine; sodium carbonate; In dichloromethane; acetonitrile; 1: Bromination / 2: Substitution;
DOI:10.1021/ja994212b

Reference yield:

: 20357-25-9
6-nitroveratraldehyde

: 113430-91-4
1-(2-nitro-4,5-dimethoxyphenyl)-N,N,N',N'-tetrakis<(ethoxycarbonyl)methyl>-1,2-ethanediamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium bis(trimethylsilyl)amide / tetrahydrofuran / 1 h / 0 °C

1.2: 43 percent / tetrahydrofuran / 20 °C

2.1: 88 percent / Br₂ / CH₂Cl₂

3.1: 12 percent / Na₂CO₃ / acetonitrile / Heating

With bromine; sodium hexamethyldisilazane; sodium carbonate; In tetrahydrofuran; dichloromethane; acetonitrile; 1.1: deprotonation / 1.2: Wittig reaction / 2.1: Bromination / 3.1: Substitution;
DOI:10.1021/ja994212b