4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid

Base Information

Chemical Name:4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid
CAS No.:1342805-80-4
Molecular Formula:C₁₅H₁₀O₇S₄
Molecular Weight:430.504
Hs Code.:

Synonyms:4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid

Suppliers and Price of 4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid

There total 2 articles about 4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 42574-02-7
4,5-diphenyl-1,3-dithio-4-cyclopenten-2-one

: 1342805-80-4
4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid

Guidance literature:: With sulfuric acid; sulfur trioxide; at 90 ℃;
DOI:10.1021/ja2072934

Reference yield:

: 501-65-5
diphenyl acetylene

: 1342805-80-4
4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1'-azobis(1-cyanocyclohexanenitrile) / m-xylene / Reflux

2: sulfuric acid; sulfur trioxide / water / 90 °C

With sulfuric acid; sulfur trioxide; 1,1'-azobis(1-cyanocyclohexanenitrile); In water; m-xylene;

Reference yield: 43.0%

: nickel(II) chloride hexahydrate

: 1342805-80-4
4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid

: C₂₈H₂₀NiO₁₂S₈

Guidance literature:: 4,4'-(2-oxo-1,3-dithiole-4,5-diyl)dibenzenesulfonic acid; With tetramethyl ammoniumhydroxide; In tetrahydrofuran; methanol; water; for 0.5h;

nickel(II) chloride hexahydrate; In tetrahydrofuran; methanol; water; for 6h;

With iodine; In tetrahydrofuran; methanol; water; at 20 ℃;