(2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol

Base Information

• Chemical Name: (2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol
• CAS No.: 1011256-27-1
• Molecular Formula: C₄₆H₅₄N₂O₂
• Molecular Weight: 666.947

Synonyms:(2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol

Chemical Property of (2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol

Chemical Property:

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Technology Process of (2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol

There total 2 articles about (2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

(2S,3S,4S,5S)-1-cyclohexyl-2,5-bis(dibenzylamino)-4-hydroxy-6-phenylhexan-3-yl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate (1011256-21-5) → (2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol (1011256-27-1)

Guidance literature:

(2S,3S,4S,5S)-1-cyclohexyl-2,5-bis(dibenzylamino)-4-hydroxy-6-phenylhexan-3-yl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate; With methanesulfonic acid; In methanol; for 16h; Heating;

With lithium hydroxide; water; In 1,4-dioxane; methanol; for 2h; Further stages.; Heating;

DOI:10.1021/jm701170f

Reference yield: 97.0%

(2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-4-hydroxy-1-phenylhexan-3-yl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate (1011256-23-7) → (2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol (1011256-27-1)

Guidance literature:

(2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-4-hydroxy-1-phenylhexan-3-yl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate; With methanesulfonic acid; In methanol; for 16h; Heating;

With lithium hydroxide; water; In 1,4-dioxane; methanol; for 2h; Further stages.; Heating;

DOI:10.1021/jm701170f

Reference yield: 55.0%

(2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-1-phenylhexane-3,4-diol (1011256-27-1) + di-tert-butyl dicarbonate (24424-99-5) → (2S,3S,4S,5S)-2,5-bis[(tert-butoxycarbonyl)amino]-6-cyclohexylhexane-1-phenylhexane-3,4-diol (1011256-30-6)

Guidance literature:

With hydrogen; palladium dihydroxide; In ethyl acetate; for 96h;

DOI:10.1021/jm701170f

upstream raw materials:

(2S,3S,4S,5S)-1-cyclohexyl-2,5-bis(dibenzylamino)-4-hydroxy-6-phenylhexan-3-yl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

(2S,3S,4S,5S)-6-cyclohexyl-2,5-bis(dibenzylamino)-4-hydroxy-1-phenylhexan-3-yl 2,2,4,4-tetramethyl-1,3-oxazolidine-3-carboxylate

Downstream raw materials:

(2S,3S,4S,5S)-2,5-bis[(tert-butoxycarbonyl)amino]-6-cyclohexylhexane-1-phenylhexane-3,4-diol

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