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Technology Process of C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2(1+)*SO3CF3(1-)=[C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2](SO3CF3)

C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2(1+)*SO3CF3(1-)=[C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2](SO3CF3)

Base Information
  • Chemical Name:C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2(1+)*SO3CF3(1-)=[C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2](SO3CF3)
  • CAS No.:1356584-33-2
  • Molecular Formula:CF3O3S*C27H35BF9OP2
  • Molecular Weight:768.389
  • Hs Code.:
C<sub>6</sub>F<sub>4</sub>B(C<sub>6</sub>F<sub>5</sub>)(OP(C<sub>2</sub>H<sub>5</sub>)3)CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2<sup>(1+)</sup>*SO<sub>3</sub>CF<sub>3</sub><sup>(1-)</sup>=[C<sub>6</sub>F<sub>4</sub>B(C<sub>6</sub>F<sub>5</sub>)(OP(C<sub>2</sub>H<sub>5</sub>)3)CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2](SO<sub>3</sub>CF<sub>3</sub>)

Synonyms:C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2(1+)*SO3CF3(1-)=[C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2](SO3CF3)

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Chemical Property of C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2(1+)*SO3CF3(1-)=[C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2](SO3CF3)
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Technology Process of C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2(1+)*SO3CF3(1-)=[C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2](SO3CF3)

There total 1 articles about C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2(1+)*SO3CF3(1-)=[C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2](SO3CF3) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

triethylphosphine oxide
597-50-2

triethylphosphine oxide

C<sub>6</sub>F<sub>5</sub>B(triflate)(C<sub>6</sub>F<sub>4</sub>P(tBu)2CH<sub>2</sub>)
1254689-45-6

C6F5B(triflate)(C6F4P(tBu)2CH2)

C<sub>6</sub>F<sub>4</sub>B(C<sub>6</sub>F<sub>5</sub>)(OP(C<sub>2</sub>H<sub>5</sub>)3)CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2<sup>(1+)</sup>*SO<sub>3</sub>CF<sub>3</sub><sup>(1-)</sup>=[C<sub>6</sub>F<sub>4</sub>B(C<sub>6</sub>F<sub>5</sub>)(OP(C<sub>2</sub>H<sub>5</sub>)3)CH<sub>2</sub>P(C(CH<sub>3</sub>)3)2](SO<sub>3</sub>CF<sub>3</sub>)
1356584-33-2

C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2(1+)*SO3CF3(1-)=[C6F4B(C6F5)(OP(C2H5)3)CH2P(C(CH3)3)2](SO3CF3)

Guidance literature:
In dichloromethane; under N2 or Ar; stirred at room temp. for 12 h; concd. under reduced pressure, layered with pentane, crystd. for 1 d, crystals isolated by decantation, cryst. material washed with hexane 4 times, dried (vac.) for 6 h; elem. anal.;
DOI:10.1002/ejic.201101098
upstream raw materials:

triethylphosphine oxide

C6F5B(triflate)(C6F4P(tBu)2CH2)

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