Technology Process of C17H15BrO2S
There total 3 articles about C17H15BrO2S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethylamine;
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide;
In
N,N-dimethyl-formamide;
at 20 ℃;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: aluminum (III) chloride; bromine / dichloromethane
2: toluene-4-sulfonic acid
3: n-butyllithium; iodine / diethyl ether
4: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide
With
aluminum (III) chloride; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; bromine; iodine; toluene-4-sulfonic acid; triethylamine;
In
diethyl ether; dichloromethane; N,N-dimethyl-formamide;
1: Friedel Crafts bromination;
DOI:10.1016/j.bmcl.2011.07.057
- Guidance literature:
-
Multi-step reaction with 2 steps
1: n-butyllithium; iodine / diethyl ether
2: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / N,N-dimethyl-formamide
With
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; n-butyllithium; iodine; triethylamine;
In
diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/j.bmcl.2011.07.057