allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Base Information

Chemical Name:allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside
CAS No.:125946-67-0
Molecular Formula:C₃₁H₃₁NO₈
Molecular Weight:545.589
Hs Code.:

Synonyms:allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

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Technology Process of allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

There total 3 articles about allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 89067-86-7
allyl 3-O-benzyl-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 150-76-5
4-methoxy-phenol

: 125946-67-0
allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With triphenylphosphine; diethylazodicarboxylate; In dichloromethane; at 20 ℃; for 24h;
DOI:10.1016/0008-6215(90)84222-G

Reference yield: 84.0%

: 150-76-5
4-methoxy-phenol

: 89067-86-7
2-((2R,4R,5S,6R)-2-Allyloxy-4-benzyloxy-5-hydroxy-6-hydroxymethyl-tetrahydro-pyran-3-yl)-isoindole-1,3-dione

: 125946-67-0
allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: With Ph₃P-diethyl azodicarboxylate; In dichloromethane;
DOI:10.1016/S0040-4039(00)99376-6

Reference yield:

: 129445-36-9
allyl 3-O-benzyl-4,6-O-benzylidene-2-deoxy-2-phthalimido-β-D-glucopyranoside

: 125946-67-0
allyl 3-O-benzyl-2-deoxy-6-O-p-methoxyphenyl-2-phthalimido-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 79 percent / 80percent aq. CH₃COOH / 1.5 h / 80 °C

2: 84 percent / Ph₃P, diethyl azodicarboxylate / CH₂Cl₂ / 24 h / 20 °C

With acetic acid; triphenylphosphine; diethylazodicarboxylate; In dichloromethane;
DOI:10.1016/0008-6215(90)84222-G