2-bromo-9,10-dihydro-9,10-dimethoxy-9,10-<1',2'>-benzenoanthracene

Base Information

Chemical Name:2-bromo-9,10-dihydro-9,10-dimethoxy-9,10-<1',2'>-benzenoanthracene
CAS No.:103438-71-7
Molecular Formula:C₂₂H₁₇BrO₂
Molecular Weight:393.28
Hs Code.:

Synonyms:2-bromo-9,10-dihydro-9,10-dimethoxy-9,10-<1',2'>-benzenoanthracene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-bromo-9,10-dihydro-9,10-dimethoxy-9,10-<1',2'>-benzenoanthracene

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Technology Process of 2-bromo-9,10-dihydro-9,10-dimethoxy-9,10-<1',2'>-benzenoanthracene

There total 1 articles about 2-bromo-9,10-dihydro-9,10-dimethoxy-9,10-<1',2'>-benzenoanthracene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 572-83-8
2-bromoanthracene-9,10-dione

: 103438-71-7
2-bromo-9,10-dihydro-9,10-dimethoxy-9,10-<1',2'>-benzenoanthracene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) sodium dithionite, water 2.) aq. NaOH / 1.) C₂H₅OH, H₂O, reflux, 45 min, 2.) 25 deg C, 2 h

2: 1.) isoamyl nitrite, anthranilic acid / 1.) THF, reflux, 1,5 h, 2.) xylene, reflux, 1 h

With sodium hydroxide; sodium dithionite; water; anthranilic acid; isopentyl nitrite;
DOI:10.1021/jo00368a010

Reference yield:

: 917-95-3
t-butylnitrite

: 103438-71-7
2-bromo-9,10-dihydro-9,10-dimethoxy-9,10-<1',2'>-benzenoanthracene

: 103438-73-9
N-<2-(9,10-dihydro-9,10-dimethoxy-9,10<1',2'>-benzenoanthracenyl)>-N-tert-butylhydroxylamine

: 97634-96-3
2-<9,10-dihydro-9,10-dimethoxy-9,10<1',2'>-benzenoanthracenyl> tert-butyl nitroxide

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) ether, hexane, 0 - 5 deg C, 2 h, and 25 deg C, 1 h, 2.) ether, hexane, 25 deg C, 15 h;
DOI:10.1021/jo00368a010