1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol

Base Information

Chemical Name:1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol
CAS No.:1621176-47-3
Molecular Formula:C₁₆H₁₃Br₄N₃O₂
Molecular Weight:598.914
Hs Code.:

Synonyms:1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol

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Chemical Property of 1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol

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Technology Process of 1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol

There total 4 articles about 1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 17374-26-4
4,5,6,7-tetrabromobenzotriazole

: 51699-51-5
3-(3-methoxyphenyl)-3-hydroxypropyl 4-methylbenzenesulfonate

: 1621176-47-3
1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol

Guidance literature:: 4,5,6,7-tetrabromobenzotriazole; With potassium carbonate; In acetone; acetonitrile; for 3h; Inert atmosphere; Reflux;

3-(3-methoxyphenyl)-3-hydroxypropyl 4-methylbenzenesulfonate; In acetone; acetonitrile; for 48h; Inert atmosphere; Reflux;
DOI:10.1016/j.ejmech.2014.07.019

Reference yield:

: 779-81-7
methyl 3-(3-methoxyphenyl)-3-oxopropanoate

: 1621176-47-3
1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium tetrahydroborate / methanol / 12 h / Inert atmosphere; Reflux

2.1: triethylamine; dmap / dichloromethane / 0.25 h / -15 °C / Inert atmosphere

2.2: 14 h / -15 - 20 °C / Inert atmosphere

3.1: potassium carbonate / acetone; acetonitrile / 3 h / Inert atmosphere; Reflux

3.2: 48 h / Inert atmosphere; Reflux

With dmap; sodium tetrahydroborate; potassium carbonate; triethylamine; In methanol; dichloromethane; acetone; acetonitrile;
DOI:10.1016/j.ejmech.2014.07.019

Reference yield:

: 95-14-7,27556-51-0
1,2,3-Benzotriazole

: 1621176-47-3
1-(3-methoxyphenyl)-3-(4,5,6,7-tetrabromo-2H-benzotriazol-2-yl)propan-1-ol

Guidance literature:: Multi-step reaction with 2 steps

1.1: nitric acid; bromine / 49 h / 60 - 80 °C / Inert atmosphere; Irradiation

2.1: potassium carbonate / acetone; acetonitrile / 3 h / Inert atmosphere; Reflux

2.2: 48 h / Inert atmosphere; Reflux

With bromine; nitric acid; potassium carbonate; In acetone; acetonitrile;
DOI:10.1016/j.ejmech.2014.07.019