methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate

Base Information

Chemical Name:methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate
CAS No.:1350651-16-9
Molecular Formula:C₂₉H₃₄N₂O₅
Molecular Weight:490.599
Hs Code.:

Synonyms:methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate

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Chemical Property of methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate

Chemical Property:

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Technology Process of methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate

There total 6 articles about methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3946-32-5
suberic acid monomethyl ester

: C₂₀H₂₀N₂O₂

: 1350651-16-9
methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;

Reference yield:

: 134-32-7
1-amino-naphthalene

: 1350651-16-9
methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate

Guidance literature:: Multi-step reaction with 6 steps

1: methanol / 20 °C / Inert atmosphere

2: methanol; sodium tetrahydroborate / 0.17 h

3: 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

4: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

5: trifluoroacetic acid / 0.5 h / 20 °C

6: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With 1H-imidazole; methanol; sodium tetrahydroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In methanol; dichloromethane;

Reference yield:

: 1350651-83-0
C₁₂H₁₁NO

: 1350651-16-9
methyl 8-(4-(2-((2-hydroxyethyl)(naphthalen-1-yl)amino)-2-oxoethyl)phenylamino)-8-oxooctanoate

Guidance literature:: Multi-step reaction with 5 steps

1: methanol; sodium tetrahydroborate / 0.17 h

2: 1H-imidazole / dichloromethane / 20 °C / Inert atmosphere

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4: trifluoroacetic acid / 0.5 h / 20 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

With 1H-imidazole; methanol; sodium tetrahydroborate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; In dichloromethane;