4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide

Base Information

Chemical Name:4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide
CAS No.:1295300-21-8
Molecular Formula:C₁₉H₁₅N₃O₄S
Molecular Weight:381.412
Hs Code.:

Synonyms:4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide

Suppliers and Price of 4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide

There total 4 articles about 4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1321626-12-3
4-[(1,3-dioxo-1H-benzo[de]isoquinolin-2(3H)-yl)methyl]benzenesulphonyl chloride

: 1295300-21-8
4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; at 0 ℃;
DOI:10.1016/j.bmc.2011.05.056

Reference yield:

: 81-84-5
1,8-Naphthalic anhydride

: 1295300-21-8
4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol / 6 h / Reflux

2: chlorosulfonic acid / 50 °C / Cooling

3: hydrazine hydrate / ethanol / 0 °C

With chlorosulfonic acid; hydrazine hydrate; In ethanol;
DOI:10.1016/j.bmc.2011.05.056

Reference yield:

: 2896-24-4
N-benzyl-1,8-naphthalimide

: 1295300-21-8
4-[(1,3-dioxo-1H-benzo[de]isoquinoline-2(3H)-yl)methyl]benzenesulphonyl hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: chlorosulfonic acid / 50 °C / Cooling

2: hydrazine hydrate / ethanol / 0 °C

With chlorosulfonic acid; hydrazine hydrate; In ethanol;
DOI:10.1016/j.bmc.2011.05.056