(Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate

Base Information

Chemical Name:(Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate
CAS No.:1310740-29-4
Molecular Formula:C₂₉H₄₂FNO₃Si
Molecular Weight:499.741
Hs Code.:

Synonyms:(Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate

Suppliers and Price of (Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate

Chemical Property:

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Technology Process of (Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate

There total 6 articles about (Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: C₂₄H₃₄FNOSi

: 1310740-29-4
(Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 39h; Inert atmosphere;
DOI:10.1016/j.tetlet.2011.03.148

Reference yield:

: 1310740-31-8
C₂₆H₃₃Cl₃FNO₂Si

: 1310740-29-4
(Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 5,5-dimethyl-1,3-cyclohexadiene / 3.5 h / 140 °C / Inert atmosphere

2: water; sodium hydroxide / ethanol / 5 h / 20 °C / Inert atmosphere

3: triethylamine / dichloromethane / 39 h / 20 °C / Inert atmosphere

With water; triethylamine; sodium hydroxide; In 5,5-dimethyl-1,3-cyclohexadiene; ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.03.148

Reference yield:

: 1310740-28-3
(Z)-N-(8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-yl)-2,2,2-trichloroacetamide

: 1310740-29-4
(Z)-tert-butyl 8-(tert-butyldiphenylsilyloxy)-5-fluorooct-5-en-4-ylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: water; sodium hydroxide / ethanol / 5 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 39 h / 20 °C / Inert atmosphere

With water; triethylamine; sodium hydroxide; In ethanol; dichloromethane;
DOI:10.1016/j.tetlet.2011.03.148