methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside

Base Information

Chemical Name:methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside
CAS No.:659722-22-2
Molecular Formula:C₃₀H₃₅N₃O₅SSi
Molecular Weight:577.777
Hs Code.:

Synonyms:methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside

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Chemical Property of methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside

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Technology Process of methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside

There total 4 articles about methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1233319-81-7
methyl 2-azido-3-O-benzoyl-2-deoxy-1-thio-β-D-allopyranoside

: 58479-61-1
tert-butylchlorodiphenylsilane

: 659722-22-2
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside

Guidance literature:: With 1H-imidazole; In dichloromethane; at 40 ℃; for 1h; Inert atmosphere;
DOI:10.1071/CH09480

Reference yield:

: C₁₅H₁₉N₃O₆S₂

: 659722-22-2
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: dimethyl sulfoxide / 140 °C

2: toluene-4-sulfonic acid; water / acetonitrile; methanol

3: 1H-imidazole / dichloromethane / 1 h / Reflux

With 1H-imidazole; water; toluene-4-sulfonic acid; In methanol; dichloromethane; dimethyl sulfoxide; acetonitrile;

Reference yield:

: 1421664-61-0
C₂₁H₂₁N₃O₅S

: 659722-22-2
methyl 2-azido-3-O-benzoyl-6-O-tert-butyldiphenylsilyl-2-deoxy-1-thio-β-D-allopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: toluene-4-sulfonic acid; water / acetonitrile; methanol

2: 1H-imidazole / dichloromethane / 1 h / Reflux

With 1H-imidazole; water; toluene-4-sulfonic acid; In methanol; dichloromethane; acetonitrile;