O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose

Base Information

Chemical Name:O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose
CAS No.:126151-76-6
Molecular Formula:C₄₀H₅₁NO₂₂
Molecular Weight:897.838
Hs Code.:

O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose

Synonyms:O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose

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Chemical Property of O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose

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Technology Process of O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose

There total 7 articles about O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 3866-62-4,3964-13-4,56822-48-1,56822-49-2,78136-22-8,80300-30-7,80300-97-6,83462-68-4,83462-69-5,94943-10-9
1-O-acetyl-2,3,4,6-tetra-O-benzyl-β-D-galactopyranoside

: 126151-76-6
O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: H₂, acetic acid / 5percent Pd/C / 3 h / 760 Torr

2: 82 percent / p-toluenesulfonic acid / acetonitrile / 0.5 h

3: silver trifluoromethanesulfonate, 2,6-di-tert-butylpyridine / tetrahydrofuran / 5 h / -55 - 0 °C

4: acetic acid, water / 1.5 h / 45 °C

5: pyridine, 4-dimethylaminopyridine / 24 h / 22 °C

With pyridine; dmap; 2,6-di-tert-butyl-pyridine; water; hydrogen; silver trifluoromethanesulfonate; toluene-4-sulfonic acid; acetic acid; palladium on activated charcoal; In tetrahydrofuran; acetonitrile;
DOI:10.1016/0008-6215(93)84162-Y

Reference yield:

: 113757-77-0
benzyl (5-acetamido-4,7,8,9-tetra-O-acetyl-2-chloro-3,5-dideoxy-D-glycero-α-D-galacto-non-2-ulpyranosid)onate

: 126151-76-6
O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: silver trifluoromethanesulfonate, 2,6-di-tert-butylpyridine / tetrahydrofuran / 5 h / -55 - 0 °C

2: acetic acid, water / 1.5 h / 45 °C

3: pyridine, 4-dimethylaminopyridine / 24 h / 22 °C

With pyridine; dmap; 2,6-di-tert-butyl-pyridine; water; silver trifluoromethanesulfonate; acetic acid; In tetrahydrofuran;
DOI:10.1016/0008-6215(93)84162-Y

Reference yield:

: 126151-75-5
1-O-acetyl-4,6-O-p-methoxybenzylidene-β-D-galactopyranose

: 126151-76-6
O-(benzyl 5-acetamido-4,7,8,9-tetra-O-acetyl-3,5-dideoxy-D-glycero-α-D-galacto-2-nonulopyranosylonate)-(2<*>3)-1,2,4,6-tetra-O-acetyl-β-D-galactopyranose

Guidance literature:: Multi-step reaction with 3 steps

1: silver trifluoromethanesulfonate, 2,6-di-tert-butylpyridine / tetrahydrofuran / 5 h / -55 - 0 °C

2: acetic acid, water / 1.5 h / 45 °C

3: pyridine, 4-dimethylaminopyridine / 24 h / 22 °C

With pyridine; dmap; 2,6-di-tert-butyl-pyridine; water; silver trifluoromethanesulfonate; acetic acid; In tetrahydrofuran;
DOI:10.1016/0008-6215(93)84162-Y