cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine

Base Information

• Chemical Name: cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine
• CAS No.: 866022-67-5
• Molecular Formula: C₃₂H₄₀NO₂P
• Molecular Weight: 501.649
• Mol file: 866022-67-5.mol

Synonyms:cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine

Chemical Property of cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine

There total 3 articles about cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(R)-N-cyclododecylphenethylamine + 2,2'-dihydroxybiphenyl (1806-29-7) → cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine (866022-67-5)

Guidance literature:

(R)-N-cyclododecylphenethylamine; With triethylamine; phosphorus trichloride; In tetrahydrofuran;

2,2'-dihydroxybiphenyl; In tetrahydrofuran; at 0 - 20 ℃; for 18h;

Reference yield:

biphenyl-2,2'-diol + (R)-N-cyclododecylphenethylamine → cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine (866022-67-5)

Guidance literature:

(R)-N-cyclododecylphenethylamine; With triethylamine; phosphorus trichloride; In tetrahydrofuran; at 20 ℃; for 3h;

biphenyl-2,2'-diol; In tetrahydrofuran; at 20 ℃; for 18h;

DOI:10.1021/ja054331t

Reference yield:

→ cyclododecyl-(5,7-dioxa-6-phospha-dibenzo[a,c]cyclohepten-6-yl)-(1-phenyl-ethyl)-amine (866022-67-5)

Guidance literature:

upstream raw materials:

2,2'-dihydroxybiphenyl