C₅₂H₆₆Cl₃N₉O₁₄

Base Information

Chemical Name:C₅₂H₆₆Cl₃N₉O₁₄
CAS No.:87329-66-6
Molecular Formula:C₅₂H₆₆Cl₃N₉O₁₄
Molecular Weight:1147.51
Hs Code.:

C<sub>52</sub>H<sub>66</sub>Cl<sub>3</sub>N<sub>9</sub>O<sub>14</sub>

Synonyms:C₅₂H₆₆Cl₃N₉O₁₄

Suppliers and Price of C₅₂H₆₆Cl₃N₉O₁₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₆₆Cl₃N₉O₁₄

Chemical Property:

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Technology Process of C₅₂H₆₆Cl₃N₉O₁₄

There total 11 articles about C₅₂H₆₆Cl₃N₉O₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58272-94-9
H-Gly-NHNH-Troc

: 87329-66-6
C₅₂H₆₆Cl₃N₉O₁₄

Guidance literature:: Multi-step reaction with 10 steps

1: 65 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

2: TFA, anisole

3: 71 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

4: TFA, anisole

5: 71 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

6: TFA, anisole

7: 85 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

8: TFA, anisole

9: 83 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

10: TFA, anisole

With 4-methyl-morpholine; methoxybenzene; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; 2-hydroxybenzothiazole; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.31.1320

Reference yield:

: 83443-90-7
Boc-Gly-NHNH-Troc

: 87329-66-6
C₅₂H₆₆Cl₃N₉O₁₄

Guidance literature:: Multi-step reaction with 11 steps

1: TFA, anisole

2: 65 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

3: TFA, anisole

4: 71 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

5: TFA, anisole

6: 71 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

7: TFA, anisole

8: 85 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

9: TFA, anisole

10: 83 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

11: TFA, anisole

With 4-methyl-morpholine; methoxybenzene; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; 2-hydroxybenzothiazole; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.31.1320

Reference yield:

: N'-[2-((S)-2-Amino-4-methyl-pentanoylamino)-acetyl]-hydrazinecarboxylic acid 2,2,2-trichloro-ethyl ester

: 87329-66-6
C₅₂H₆₆Cl₃N₉O₁₄

Guidance literature:: Multi-step reaction with 8 steps

1: 71 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

2: TFA, anisole

3: 71 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

4: TFA, anisole

5: 85 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

6: TFA, anisole

7: 83 percent / hydroxybenzothiazole, 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, N-methylmorpholine / dimethylformamide / 0 deg C 3 h; room temperature 12 h

8: TFA, anisole

With 4-methyl-morpholine; methoxybenzene; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; trifluoroacetic acid; 2-hydroxybenzothiazole; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.31.1320