4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside

Base Information

Chemical Name:4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside
CAS No.:1164151-42-1
Molecular Formula:C₃₀H₂₈F₃NO₉S₂
Molecular Weight:667.681
Hs Code.:

Synonyms:4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside

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Chemical Property of 4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside

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Technology Process of 4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside

There total 1 articles about 4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 358-23-6
trifluoromethylsulfonic anhydride

: 1164151-33-0
4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-1-thio-β-D-galactopyranoside

: 1164151-42-1
4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside

Guidance literature:: With pyridine; In dichloromethane; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.067

Reference yield: 33.4%

: 51450-09-0
2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose

: 1164151-42-1
4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside

: 1164151-52-3
4-methylphenyl 2-acetamido-4-S-(2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-β-D-glucopyranosyl)-3,6-di-O-benzoyl-2-deoxy-1,4-dithio-β-D-glucopyranoside

Guidance literature:: 2-acetamido-3,4,6-tri-O-acetyl-2-deoxy-1-thio-β-D-glucopyranose; With sodium hydride; In tetrahydrofuran; mineral oil; for 0.0833333h; Inert atmosphere;

4-methylphenyl 2-acetamido-3,6-di-O-benzoyl-2-deoxy-4-O-trifluormethane-sulfonyl-1-thio-β-D-galactopyranoside; With 18-crown-6 ether; In tetrahydrofuran; mineral oil; at 20 ℃; for 6h; Inert atmosphere;
DOI:10.1016/j.tet.2009.03.067