4-[(3,3'-dimethyl[1,1'-biphenyl]-4-yl)oxy]-5-(4-morpholinyl)phthalonitrile

Base Information

Chemical Name:4-[(3,3'-dimethyl[1,1'-biphenyl]-4-yl)oxy]-5-(4-morpholinyl)phthalonitrile
CAS No.:696619-39-3
Molecular Formula:C₂₆H₂₃N₃O₂
Molecular Weight:409.488
Hs Code.:
Mol file:696619-39-3.mol

Synonyms:4-(morpholin-4-yl)-5-((3,3'-dimethyl(1,1'-biphenyl)-4-yl)oxy)phthalodinitrile

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Chemical Property of 4-[(3,3'-dimethyl[1,1'-biphenyl]-4-yl)oxy]-5-(4-morpholinyl)phthalonitrile

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Technology Process of 4-[(3,3'-dimethyl[1,1'-biphenyl]-4-yl)oxy]-5-(4-morpholinyl)phthalonitrile

There total 1 articles about 4-[(3,3'-dimethyl[1,1'-biphenyl]-4-yl)oxy]-5-(4-morpholinyl)phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 876473-48-2
3,3'-dimethyl-(1,1'-biphenyl)-4-ol

: 274924-66-2
4-morpholino-5-nitrophthalinonitrile

: 696619-39-3
4-(morpholin-4-yl)-5-((3,3'-dimethyl(1,1'-biphenyl)-4-yl)oxy)phthalodinitrile

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 130 - 140 ℃; for 3h;
DOI:10.1134/S1070363209050260

Reference yield: 41.0%

: 696619-39-3
4-(morpholin-4-yl)-5-((3,3'-dimethyl(1,1'-biphenyl)-4-yl)oxy)phthalodinitrile

: copper tetra-4-(morpholin-4-yl)-tetra-5-{[3,3'-dimethyl(1,1'-biphenyl)-4-yl]oxy}phthalocyanine

Guidance literature:: With copper(II) acetate dihydrate; urea; at 180 - 185 ℃; for 2h;
DOI:10.1134/S1070363209050260

Reference yield: 41.0%

: copper(II) acetate dihydrate

: 696619-39-3
4-(morpholin-4-yl)-5-((3,3'-dimethyl(1,1'-biphenyl)-4-yl)oxy)phthalodinitrile

: 1210913-56-6
copper tetra-4-(morpholin-4-yl)-tetra-5-((3,3'-dimethyl(1,1'-biphenyl)-4-yl)oxy)phthalocyanine

Guidance literature:: With carbamide; In neat (no solvent); the mixt. of Cu-salt, phthalodinitrile and carbamide was heated to 180-185°C and kept for 2 h; washed with 5% HCl, water, extd. with CHCl3, column chromy. in Al2O3 (CHCl3), the solvent was distilled off in vac., dried at 80°C; elem.anal.;
DOI:10.1134/S1070363209050260