12-(diphenylchlorosilyl)-1,1,4,4,7,7,10,10-octamethyloctahydro dibenzofluorene

Base Information

Chemical Name:12-(diphenylchlorosilyl)-1,1,4,4,7,7,10,10-octamethyloctahydro dibenzofluorene
CAS No.:676647-40-8
Molecular Formula:C₄₁H₄₇ClSi
Molecular Weight:603.363
Hs Code.:

Synonyms:12-(diphenylchlorosilyl)-1,1,4,4,7,7,10,10-octamethyloctahydro dibenzofluorene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 12-(diphenylchlorosilyl)-1,1,4,4,7,7,10,10-octamethyloctahydro dibenzofluorene

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Technology Process of 12-(diphenylchlorosilyl)-1,1,4,4,7,7,10,10-octamethyloctahydro dibenzofluorene

There total 3 articles about 12-(diphenylchlorosilyl)-1,1,4,4,7,7,10,10-octamethyloctahydro dibenzofluorene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.3%

: 77308-48-6
1,1,4,4,7,7,10,10-octamethyl-2,3,4,7,8,9,10,12-octahydro-1H-dibenzo[b,h]fluorene

: 80-10-4
diphenylsilyl dichloride

: 676647-40-8
12-(diphenylchlorosilyl)-1,1,4,4,7,7,10,10-octamethyloctahydro dibenzofluorene

Guidance literature:: 1,1,4,4,7,7,10,10-octamethyl-2,3,4,7,8,9,10,12-octahydro-1H-dibenzo[b,h]fluorene; With n-butyllithium; In tetrahydrofuran; hexane; for 20h; Cooling with ice;

diphenylsilyl dichloride; In tetrahydrofuran; hexane; for 44h; Concentration; Time; Cooling with ice;

Reference yield:

: 77308-48-6
1,1,4,4,7,7,10,10-octamethyl-2,3,4,7,8,9,10,12-octahydro-1H-dibenzo[b,h]fluorene

: 676647-40-8
12-(diphenylchlorosilyl)-1,1,4,4,7,7,10,10-octamethyloctahydro dibenzofluorene

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether; hexane / 20 h

2: diethyl ether; hexane / 17.5 h

In diethyl ether; hexane;
DOI:10.1039/c3dt50163a