tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate

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Chemical Name:tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate
CAS No.:1119260-84-2
Molecular Formula:C₆₉H₈₄N₂O₂Si
Molecular Weight:1001.52
Hs Code.:

Synonyms:tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate

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Chemical Property of tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate

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Technology Process of tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate

There total 1 articles about tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.2%

: 1119260-80-8
tert-butyl 4-((4-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate

: 1119260-82-0
(4-(7-bromo-9,9-dioctyl-9H-fluoren-2-yl)phenyl)trimethylsilane

: 1119260-84-2
tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; tetraethylammonium hydroxide; In water; toluene; at 80 ℃; for 14h; Inert atmosphere;
DOI:10.1021/ol8029164

Reference yield: 90.0%

: 1119260-84-2
tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate

: 1119260-86-4
C₆₁H₆₈N₂

Guidance literature:: tert-butyl 4-((4-(9,9-dioctyl-7-(4-(trimethylsilyl)phenyl)-9H-fluoren-2-yl)phenyl)(p-tolyl)amino)phenyl(p-tolyl)carbamate; With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

With sodium hydrogencarbonate; In dichloromethane; Inert atmosphere;
DOI:10.1021/ol8029164