1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one

Base Information

Chemical Name:1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one
CAS No.:1613733-72-4
Molecular Formula:C₁₅H₇BrCl₃F₃OS
Molecular Weight:478.544
Hs Code.:

Synonyms:1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one

Suppliers and Price of 1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one

There total 1 articles about 1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 859199-06-7
1-(5-bromo-4-methylthiophen-2-yl)ethan-1-one

: 158401-00-4
1-(3,4,5-trichloro-phenyl)-2,2,2-trifluoro-ethanone

: 1613733-72-4
1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one

Guidance literature:: 1-(5-bromo-4-methylthiophen-2-yl)ethan-1-one; 1-(3,4,5-trichloro-phenyl)-2,2,2-trifluoro-ethanone; With triethylamine; In tert-butyl methyl ether; at 57 ℃; for 2h; Large scale;

With thionyl chloride; In tert-butyl methyl ether; at 5 - 40 ℃; for 3h; Large scale;

Reference yield: 81.0%

: 1613733-72-4
1-(5-bromo-4-methyl-2-thienyl)-4,4,4-trifluoro-3-(3,4,5-trichlorophenyl)but-2-en-1-one

: (5S)-3-(5-bromo-4-methyl-2-thienyl)-5-(3,4,5-trichlorophenyl)-5-(trifluoromethyl)-4H-isoxazole

Guidance literature:: With hydroxylamine; (R)-[(2S)-1-[[3,5-bis(trifluoromethyl)phenyl]methyl]-5-vinyl-quinuclidin-1-ium-2-yl]-(6-methoxy-4-quinolyl)methanol bromide; sodium hydroxide; In dichloromethane; water; at -15 - 20 ℃; for 7h; Reagent/catalyst; Solvent; Temperature; Inert atmosphere;