32-hydroxydotriacontanoic acid

Base Information

• Chemical Name: 32-hydroxydotriacontanoic acid
• CAS No.: 52900-19-3
• Molecular Formula: C₃₂H₆₄O₃
• Molecular Weight: 496.858

Synonyms:32-hydroxydotriacontanoic acid

Chemical Property of 32-hydroxydotriacontanoic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 32-hydroxydotriacontanoic acid

There total 1 articles about 32-hydroxydotriacontanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

16-bromohexadecan-1-ol (59101-28-9) → 32-hydroxydotriacontanoic acid (52900-19-3)

Guidance literature:

Multi-step reaction with 9 steps

1.1: pyridinium p-toluenesulfonate / chloroform / 3 h / Reflux; Inert atmosphere

2.1: N,N-dimethyl-formamide / 6 h / 90 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: dimethyl sulfoxide; oxalyl dichloride; triethylamine / dichloromethane / -55 - 20 °C / Inert atmosphere

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 1.5 h / -20 °C / Inert atmosphere; Reflux

5.2: -20 - 20 °C / Inert atmosphere

6.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 5 h / 0 °C / Inert atmosphere; Reflux

7.1: palladium 10% on activated carbon; hydrogen / ethyl acetate / 20 °C

8.1: pyridinium p-toluenesulfonate / methanol / 48 h / 20 °C

9.1: sodium hydroxide / methanol / 24 h / Reflux

9.2: pH 1

With dmap; lithium aluminium tetrahydride; oxalyl dichloride; palladium 10% on activated carbon; hydrogen; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; chloroform; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1021/acs.orglett.5b02816

upstream raw materials:

16-bromohexadecan-1-ol

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 52900-19-3 32-hydroxydotriacontanoic acid

Send

Send

Metric Ton KG G Pound L ML

Send

Send