Technology Process of C38H48FN5O9S
There total 9 articles about C38H48FN5O9S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
caesium carbonate;
In
dimethyl sulfoxide;
at 60 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 0 - 20 °C
2.1: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 0 °C
2.2: 0 - 20 °C
3.1: caesium carbonate / dimethyl sulfoxide / 60 °C
With
carbon tetrabromide; caesium carbonate; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: potassium carbonate / acetonitrile / 12 h / Reflux
2.1: sodium tetrahydroborate / tetrahydrofuran / 0.25 h / 65 °C
2.2: 4.5 h / 65 °C
3.1: carbon tetrabromide; triphenylphosphine / dichloromethane / 2 h / 0 - 20 °C
4.1: lithium hexamethyldisilazane / N,N-dimethyl-formamide; tetrahydrofuran / 0.5 h / 0 °C
4.2: 0 - 20 °C
5.1: caesium carbonate / dimethyl sulfoxide / 60 °C
With
sodium tetrahydroborate; carbon tetrabromide; potassium carbonate; caesium carbonate; triphenylphosphine; lithium hexamethyldisilazane;
In
tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; acetonitrile;