C₂₂H₂₁⁽³⁾HN₄O₂

Base Information

Chemical Name:C₂₂H₂₁⁽³⁾HN₄O₂
CAS No.:131068-58-1
Molecular Formula:C₂₂H₂₂N₄O₂
Molecular Weight:376.434
Hs Code.:

C<sub>22</sub>H<sub>21</sub><sup>(3)</sup>HN<sub>4</sub>O<sub>2</sub>

Synonyms:C₂₂H₂₁⁽³⁾HN₄O₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₂H₂₁⁽³⁾HN₄O₂

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Technology Process of C₂₂H₂₁⁽³⁾HN₄O₂

There total 10 articles about C₂₂H₂₁⁽³⁾HN₄O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 132083-91-1
C₂₂H₂₂⁽³⁾HNO₃

: 131068-58-1
C₂₂H₂₁⁽³⁾HN₄O₂

Guidance literature:: With ZnN₆*2Pyr; triphenylphosphine; diethylazodicarboxylate; In toluene;

Reference yield:

: 26866-40-0
3,5'-O-dibenzylpyridoxal

: 131068-58-1
C₂₂H₂₁⁽³⁾HN₄O₂

Guidance literature:: Multi-step reaction with 4 steps

1: 85 percent / NaBT₄ / tetrahydrofuran

2: 94 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂

3: 85 percent / (S)-alpine-borane / tetrahydrofuran

4: 93 percent / DEAD, ZnN₆*2Pyr, Ph₃P / toluene

With sodium boron [ 3H]hydride; (-)-(S)-alpine-borane; ZnN₆*2Pyr; sodium acetate; triphenylphosphine; pyridinium chlorochromate; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 26864-21-1
5'-O-benzylpyridoxine

: 131068-58-1
C₂₂H₂₁⁽³⁾HN₄O₂

Guidance literature:: Multi-step reaction with 6 steps

1: NaOMe / methanol

2: pyridinium chlorochromate, NaOAc / CH₂Cl₂

3: 85 percent / NaBT₄ / tetrahydrofuran

4: 94 percent / pyridinium chlorochromate, NaOAc / CH₂Cl₂

5: 85 percent / (S)-alpine-borane / tetrahydrofuran

6: 93 percent / DEAD, ZnN₆*2Pyr, Ph₃P / toluene

With sodium boron [ 3H]hydride; (-)-(S)-alpine-borane; ZnN₆*2Pyr; sodium methylate; sodium acetate; triphenylphosphine; pyridinium chlorochromate; diethylazodicarboxylate; In tetrahydrofuran; methanol; dichloromethane; toluene;