(C₆H₄(CH₃)2(CH(CO₂CH₂CH₃)SO₂C₆H₅)Si(CH₃)3)Fe(CO)3

Base Information

Chemical Name:(C₆H₄(CH₃)2(CH(CO₂CH₂CH₃)SO₂C₆H₅)Si(CH₃)3)Fe(CO)3
CAS No.:81095-47-8
Molecular Formula:C₂₄H₃₀FeO₇SSi
Molecular Weight:546.497
Hs Code.:

(C<sub>6</sub>H<sub>4</sub>(CH<sub>3</sub>)2(CH(CO<sub>2</sub>CH<sub>2</sub>CH<sub>3</sub>)SO<sub>2</sub>C<sub>6</sub>H<sub>5</sub>)Si(CH<sub>3</sub>)3)Fe(CO)3

Synonyms:(C₆H₄(CH₃)2(CH(CO₂CH₂CH₃)SO₂C₆H₅)Si(CH₃)3)Fe(CO)3

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Chemical Property of (C₆H₄(CH₃)2(CH(CO₂CH₂CH₃)SO₂C₆H₅)Si(CH₃)3)Fe(CO)3

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Technology Process of (C₆H₄(CH₃)2(CH(CO₂CH₂CH₃)SO₂C₆H₅)Si(CH₃)3)Fe(CO)3

There total 2 articles about (C₆H₄(CH₃)2(CH(CO₂CH₂CH₃)SO₂C₆H₅)Si(CH₃)3)Fe(CO)3 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 81064-35-9
(C₆H₄(CH₃)2Si(CH₃)3)Fe(CO)3⁽¹⁺⁾*PF₆^(1-)=(C₆H₄(CH₃)2Si(CH₃)3)Fe(CO)3PF₆

: 75850-40-7
ethyl (phenylsulfonyl)sodioacetate

: 81095-47-8
(C₆H₄(CH₃)2(CH(CO₂CH₂CH₃)SO₂C₆H₅)Si(CH₃)3)Fe(CO)3

Guidance literature:: In not given; inseparable mixt. of diastereomers was obtained; identified by elem. anal. and mass spectra;
DOI:10.1021/om00065a018

Reference yield: 69.5%

: 81064-35-9
(C₆H₄(CH₃)2Si(CH₃)3)Fe(CO)3⁽¹⁺⁾*PF₆^(1-)=(C₆H₄(CH₃)2Si(CH₃)3)Fe(CO)3PF₆

: 7605-30-3
ethyl 2-phenylsulfonylacetate

: 81095-47-8
(C₆H₄(CH₃)2(CH(CO₂CH₂CH₃)SO₂C₆H₅)Si(CH₃)3)Fe(CO)3

Guidance literature:: With sodium hydride; In tetrahydrofuran; a THF soln. of acetate was added dropwise under N2 to a stirred suspn. of NaH in THF, resulting soln. was stirred at room temp. for 5 min, added dropwise under N2 to a stirred THF suspn. of Fe-complex, mixt. was stirred at room temp. for 30 min; poured into water, layers were sepd., aq. layer was extd. with light petroleum, combined org. layers dried, evapd., residue was chromd. on silica gel (eluent benzene), recrystd. from hot hexane to give an unseparable mixt. of diastereomers;