N,N''-(2-methoxy-1,3-phenylene)bis

Base Information

Chemical Name:N,N''-(2-methoxy-1,3-phenylene)bis
CAS No.:91084-87-6
Molecular Formula:C₃₁H₃₆N₄O₇
Molecular Weight:576.649
Hs Code.:

N,N''-(2-methoxy-1,3-phenylene)bis<N'-(2,2,6-trimethyl-4H-1,3-benzodioxin-8-yl)urea>

Synonyms:N,N''-(2-methoxy-1,3-phenylene)bis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N,N''-(2-methoxy-1,3-phenylene)bis

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Technology Process of N,N''-(2-methoxy-1,3-phenylene)bis

There total 1 articles about N,N''-(2-methoxy-1,3-phenylene)bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 129125-41-3
1,3-Diisocyanato-2-methoxy-benzene

: 91084-85-4
8-amino-2,2,6-trimethyl-4H-1,3-benzodioxin

: 91084-87-6
N,N''-(2-methoxy-1,3-phenylene)bis

Guidance literature:: In toluene; at 85 ℃; for 3h;
DOI:10.1021/ja00329a058

Reference yield:

: 91084-87-6
N,N''-(2-methoxy-1,3-phenylene)bis

: 91084-78-5
1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / NaOH, benzyltriethylammonium bromide / benzene; H₂O / 20 h / 50 °C

2: 90 percent / Dowex-50 sulfonic acid resin / methanol / 1.33 h

3: 38 percent / sodium hydroxide / tetrahydrofuran; H₂O / 1 h / 60 °C

With sodium hydroxide; Dowex-50 sulfonic acid resin; benzyltriethylammonium bromide; In tetrahydrofuran; methanol; water; benzene;
DOI:10.1021/ja00329a058

Reference yield:

: 91084-87-6
N,N''-(2-methoxy-1,3-phenylene)bis

: 91110-52-0
1,1'-(2-methoxy-1,3-phenylene)bis-2(1H)-pyrimidinone>

Guidance literature:: Multi-step reaction with 2 steps

1: 37 percent / NaOH, benzyltriethylammonium bromide / benzene; H₂O / 20 h / 50 °C

2: 90 percent / Dowex-50 sulfonic acid resin / methanol / 1.33 h

With sodium hydroxide; Dowex-50 sulfonic acid resin; benzyltriethylammonium bromide; In methanol; water; benzene;
DOI:10.1021/ja00329a058