1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl

Base Information

Chemical Name:1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl
CAS No.:73864-56-9
Molecular Formula:C₂₄H₂₈N₂O₉
Molecular Weight:488.494
Hs Code.:

Synonyms:1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl

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Chemical Property of 1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl

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Technology Process of 1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl

There total 6 articles about 1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 80581-77-7
1,2,3-tri-O-acetyl-5-O-benzoyl-3-C-butyl-α,β-D-ribofuranose

: 3442-82-8
1,3-bis(trimethylsilyl)uracil

: 73864-56-9
1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl

Guidance literature:: With tin(IV) chloride; In acetonitrile; for 40h; Ambient temperature;
DOI:10.1016/S0008-6215(00)83835-5

Reference yield:

: 72659-81-5
3-C-butyl-1,2:5,6-di-O-isopropylidene-α-D-allofuranose

: 73864-56-9
1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl

Guidance literature:: Multi-step reaction with 5 steps

1: 88 percent / water / acetic acid / 40 h / Ambient temperature

2: 1.) sodium metaperiodate; 2.) sodium borohydride / 1.) water, 1 h, 20 deg C; 2.) ethanol, 16 h, room temp.

3: 91 percent / pyridine / 16 h / 0 °C

4: 2.) p-toluenesulfonic acid monohydrate / 1.) 90percent aq. trifluoroacetic acid, 0.5 h, room temp.; 2) chloroform, 3 d

5: 75 percent / tin tetrachloride / acetonitrile / 40 h / Ambient temperature

With sodium tetrahydroborate; sodium periodate; water; tin(IV) chloride; toluene-4-sulfonic acid; In pyridine; acetic acid; acetonitrile;
DOI:10.1016/S0008-6215(00)83835-5

Reference yield:

: 73864-49-0
3-C-butyl-1,2-O-isopropylidene-α-D-ribofuranose

: 73864-56-9
1-(2,3-di-O-acetyl-5-O-benzoyl-3-C-butyl-β-D-ribofuranosyl)uracyl

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / pyridine / 16 h / 0 °C

2: 2.) p-toluenesulfonic acid monohydrate / 1.) 90percent aq. trifluoroacetic acid, 0.5 h, room temp.; 2) chloroform, 3 d

3: 75 percent / tin tetrachloride / acetonitrile / 40 h / Ambient temperature

With tin(IV) chloride; toluene-4-sulfonic acid; In pyridine; acetonitrile;
DOI:10.1016/S0008-6215(00)83835-5