2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione

Base Information

• Chemical Name: 2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione
• CAS No.: 72849-64-0
• Molecular Formula: C₁₂H₁₀ClFN₂O₂S
• Molecular Weight: 300.741

Synonyms:2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione

Chemical Property of 2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione

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Technology Process of 2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione

There total 1 articles about 2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-fluoro-4-chlorophenyl isocyanate (69922-26-5) + ethyl thiomorpholine-3-carboxylate (58729-31-0) → 2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione (72849-64-0)

Guidance literature:

With triethylamine;

Reference yield:

2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione (72849-64-0) → 8-chloro-2-(4-chloro-2-fluoro-phenyl)-tetrahydro-imidazo[5,1-c][1,4]thiazine-1,3-dione (72850-09-0) + 8-Chloro-2-(4-chloro-2-flurorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo[5,1-c][1,4]thiazine-1,3(2H)-dione

Guidance literature:

With N-chloro-succinimide; In methylene chloride;

Reference yield:

2-(2-Fluoro-4-chlorophenyl)-5,6,8,8A-tetrahydro-1H-imidazo-[5,1-c][1,4]thiazine-1,3(2H)-dione (72849-64-0) → 2-(4-chloro-2-fluoro-phenyl)-7,7-dioxo-tetrahydro-7λ6-imidazo[5,1-c][1,4]thiazine-1,3-dione (72849-65-1)

Guidance literature:

With m-chloroperoxybenzoic acid; In dichloromethane;

upstream raw materials:

2-fluoro-4-chlorophenyl isocyanate

ethyl thiomorpholine-3-carboxylate

Downstream raw materials:

8-chloro-2-(4-chloro-2-fluoro-phenyl)-tetrahydro-imidazo[5,1-c][1,4]thiazine-1,3-dione

2-(4-chloro-2-fluoro-phenyl)-7,7-dioxo-tetrahydro-7λ⁶-imidazo[5,1-c][1,4]thiazine-1,3-dione

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