N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline

Base Information

Chemical Name:N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline
CAS No.:122350-58-7
Molecular Formula:C₂₇H₃₄N₂O₁₂
Molecular Weight:578.573
Hs Code.:

N-benzyloxycarbonyl <N<sup>1</sup>-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline

Synonyms:N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline

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Chemical Property of N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline

Chemical Property:

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Technology Process of N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline

There total 3 articles about N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 41355-50-4,51642-81-0,58484-22-3,70128-27-7,70145-20-9,94482-21-0,98300-76-6
2,3,4,6-tetra-O-acetyl-D-glucosyl-1-amine

: 1148-11-4
N-Benzyloxycarbonyl-L-proline

: 122350-58-7
N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline

Guidance literature:: With 4-methyl-morpholine; isobutyl chloroformate; In tetrahydrofuran; at -15 ℃;

Reference yield:

: 572-09-8
2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

: 122350-58-7
N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / acetone / 56 °C

2: palladium; hydrogen / methanol; ethyl acetate

3: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -15 °C

With 4-methyl-morpholine; sodium azide; hydrogen; palladium; isobutyl chloroformate; In tetrahydrofuran; methanol; ethyl acetate; acetone;

Reference yield:

: 13992-25-1
1-azido-1-deoxy-β-D-glucopyranoside tetraacetate

: 122350-58-7
N-benzyloxycarbonyl 1-2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl> proline

Guidance literature:: Multi-step reaction with 2 steps

1: palladium; hydrogen / methanol; ethyl acetate

2: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / -15 °C

With 4-methyl-morpholine; hydrogen; palladium; isobutyl chloroformate; In tetrahydrofuran; methanol; ethyl acetate;