2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyanine

Base Information

• Chemical Name: 2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyanine
• CAS No.: 1257309-60-6
• Molecular Formula: C₁₁₉H₁₁₀N₈O₈
• Molecular Weight: 1780.23

Synonyms:2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyanine

Chemical Property of 2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyanine

Chemical Property:

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Technology Process of 2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyanine

There total 1 articles about 2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyanine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 51.0%

C99H96N8O7 (948904-73-2) + 1-pyrenebutyric acid (3443-45-6) → 2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyanine (1257309-60-6)

Guidance literature:

1-pyrenebutyric acid; With dmap; dicyclohexyl-carbodiimide; In tetrahydrofuran; at 0 ℃; for 0.333333h;

C₉₉H₉₆N₈O₇; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1021/ja107131r

Reference yield: 66.0%

2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyanine (1257309-60-6) → 2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyaninate Zn(II) (1257334-97-6)

Guidance literature:

With zinc(II) chloride; In N,N-dimethyl-formamide; 1,2-dichloro-benzene; at 140 ℃; for 18h;

DOI:10.1021/ja107131r

upstream raw materials:

C₉₉H₉₆N₈O₇

1-pyrenebutyric acid

Downstream raw materials:

2,3,9,10,16,17-hexa(4-tert-butylphenoxy)-23-[p-(4-pyrenbutyryloxymethyl)phenyl]phthalocyaninate Zn(II)

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