S-2,4,6-trimethoxybenzyl 3,5-bis(prop-2-ynyloxy)benzothioate

Base Information

• Chemical Name: S-2,4,6-trimethoxybenzyl 3,5-bis(prop-2-ynyloxy)benzothioate
• CAS No.: 1227069-44-4
• Molecular Formula: C₂₃H₂₂O₆S
• Molecular Weight: 426.49
• Mol file: 1227069-44-4.mol

Synonyms:S-2,4,6-trimethoxybenzyl 3,5-bis(prop-2-ynyloxy)benzothioate

Chemical Property of S-2,4,6-trimethoxybenzyl 3,5-bis(prop-2-ynyloxy)benzothioate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of S-2,4,6-trimethoxybenzyl 3,5-bis(prop-2-ynyloxy)benzothioate

There total 1 articles about S-2,4,6-trimethoxybenzyl 3,5-bis(prop-2-ynyloxy)benzothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

3,5-bis(prop-2-yn-1-yloxy) benzoic acid (664334-21-8) + (2,4,6-trimethoxyphenyl)methanethiol (212555-23-2) → S-2,4,6-trimethoxybenzyl 3,5-bis(prop-2-ynyloxy)benzothioate (1227069-44-4)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; at 20 ℃; for 72h; Inert atmosphere;

DOI:10.1021/jm100246m

Reference yield: 63.0%

S-2,4,6-trimethoxybenzyl 3,5-bis(prop-2-ynyloxy)benzothioate (1227069-44-4) + N3-Ahx-D-Phe-cyclo(Cys-Tyr-D-Trp-Lys-Thr-Cys)-threol (1173177-25-7) → C133H172N26O30S5 (1227069-46-6)

Guidance literature:

With (+)-sodium-L-ascorbate; copper(II) sulfate; In tetrahydrofuran; water; at 100 ℃; for 0.0833333h; Microwave irradiation;

DOI:10.1021/jm100246m

upstream raw materials:

3,5-bis(prop-2-yn-1-yloxy) benzoic acid

(2,4,6-trimethoxyphenyl)methanethiol

Downstream raw materials:

C₁₃₃H₁₇₂N₂₆O₃₀S₅