3,4-xylidino-D-ribofuranoside

Base Information

Chemical Name:3,4-xylidino-D-ribofuranoside
CAS No.:111619-05-7
Molecular Formula:C₁₃H₁₉NO₄
Molecular Weight:253.298
Hs Code.:

Synonyms:3,4-xylidino-D-ribofuranoside

Suppliers and Price of 3,4-xylidino-D-ribofuranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,4-xylidino-D-ribofuranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,4-xylidino-D-ribofuranoside

There total 1 articles about 3,4-xylidino-D-ribofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.2%

: 36468-53-8
β-D-ribofuranose

: 95-64-7
4-amino-o-xylene

: 111619-05-7
3,4-xylidino-D-ribofuranoside

Guidance literature:: With ammonium chloride; In methanol; for 1h; Heating;

Reference yield: 75.0%

: 111619-05-7
3,4-xylidino-D-ribofuranoside

: 3051-94-3
3,4-dimethyl-N-ribitylaniline

Guidance literature:: With hydrogen; palladium on activated charcoal; In N,N-dimethyl-formamide; for 1h; under 3102.9 Torr;

Reference yield:

: 111619-05-7
3,4-xylidino-D-ribofuranoside

: 10-[(2S,3S,4R)-5-(tert-Butyl-diphenyl-silanyloxy)-2,3,4-tris-(tetrahydro-pyran-2-yloxy)-pentyl]-7,8-dimethyl-5,10-dihydro-4aH-pyrimido[4,5-b]quinoline-2,4-dione

Guidance literature:: Multi-step reaction with 8 steps

1: 75 percent / H₂ / 10 percent Pd/C / dimethylformamide / 1 h / 3102.9 Torr

2: 68 percent

3: 90 percent / perchloric acid / 2 h / 20 °C

4: 85 percent / POCl₃

5: 96 percent / anhydrous hydrogen chloride / methanol / 18 h / 20 °C

6: 94 percent / pyridine / 60 h

7: 87 percent / mesitylenesulphonic acid / acetonitrile / 58 h / 20 °C

8: NaBH₄ / methanol

With hydrogenchloride; sodium tetrahydroborate; perchloric acid; mesitylene sulfonic acid; hydrogen; trichlorophosphate; palladium on activated charcoal; In pyridine; methanol; N,N-dimethyl-formamide; acetonitrile;