2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester

Base Information

Chemical Name:2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester
CAS No.:264888-53-1
Molecular Formula:C₂₉H₃₇NO₈
Molecular Weight:527.615
Hs Code.:

2-<i>tert</i>-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester

Synonyms:2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester

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Chemical Property of 2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester

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Technology Process of 2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester

There total 5 articles about 2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 264888-38-2
2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(3-benzyloxy-6-hydroxy-2,4-dimethyl-phenyl)-3-methyl-butyl] ester

: 264888-53-1
2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester

Guidance literature:: With N-Bromosuccinimide; In water; acetone; for 0.25h;
DOI:10.1248/cpb.48.238

Reference yield:

: 7536-58-5,98482-77-0
BOC-L-aspartic acid 4-benzyl ester

: 264888-53-1
2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / EDC; DMAP / CH₂Cl₂ / 5 h / 20 °C

2: 98 percent / NBS / acetone; H₂O / 0.25 h

With dmap; N-Bromosuccinimide; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; water; acetone; 1: Acylation / 2: Oxidation;
DOI:10.1248/cpb.48.238

Reference yield:

: 50442-68-7
6-hydroxy-4,4,5,7-tetramethyl-3,4-dihydrocoumarin

: 264888-53-1
2-tert-butoxycarbonylamino-succinic acid 4-benzyl ester 1-[3-(2,4-dimethyl-3,6-dioxo-cyclohexa-1,4-dienyl)-3-methyl-butyl] ester

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / K₂CO₃; NaI / acetone / 20 h / Heating

2: 97 percent / LiAlH₄ / tetrahydrofuran / 7 h / 20 °C

3: 100 percent / EDC; DMAP / CH₂Cl₂ / 5 h / 20 °C

4: 98 percent / NBS / acetone; H₂O / 0.25 h

With dmap; N-Bromosuccinimide; lithium aluminium tetrahydride; potassium carbonate; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; sodium iodide; In tetrahydrofuran; dichloromethane; water; acetone; 1: Alkylation / 2: Reduction / 3: Acylation / 4: Oxidation;
DOI:10.1248/cpb.48.238