(R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride

Base Information

Chemical Name:(R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride
CAS No.:1147391-39-6
Molecular Formula:C₁₃H₂₀BNO₂*ClH
Molecular Weight:269.579
Hs Code.:

Synonyms:(R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride

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Chemical Property of (R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride

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Technology Process of (R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride

There total 1 articles about (R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 849519-42-2
(R)-1-[2-(4-bromo-phenyl)-ethyl]-2-methyl-pyrrolidine

: 1147391-39-6
(R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride

Guidance literature:: (R)-1-[2-(4-bromo-phenyl)-ethyl]-2-methyl-pyrrolidine; With n-butyllithium; In tetrahydrofuran; at -78 - -68 ℃; for 0.25h; Cooling with acetone-dry ice;

With Triisopropyl borate; In tetrahydrofuran; at -72 - 20 ℃; for 1h;

With hydrogenchloride; In tetrahydrofuran; water; Acidic conditions;

Reference yield: 98.0%

: 1147391-38-5
(R)-4-(2-oxooxazolidin-4-yl)phenyl trifluoromethanesulfonate

: 1147391-39-6
(R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride

: 1147391-40-9
(R)-4-(4'-(2-((R)-2-methylpyrrolidin-1-yl)ethyl)biphenyl-4-yl)oxazolidin-2-one

Guidance literature:: (R)-4-(2-oxooxazolidin-4-yl)phenyl trifluoromethanesulfonate; (R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride; With sodium carbonate; In water; toluene; at 21 - 33 ℃;

tetrakis(triphenylphosphine) palladium⁽⁰⁾; In water; toluene; at 20 - 90 ℃; Product distribution / selectivity; Heating / reflux;

Reference yield:

: 1147392-80-0
5-(4-bromophenyl)morpholin-3-one

: 1147391-39-6
(R)-4-(2-(2-methylpyrrolidin-1-yl)ethyl)phenylboronic acid hydrochloride

: 1147392-76-4
5-(4'-(2-((R)-2-methylpyrrolidin-1-yl)ethyl)biphenyl-4-yl)morpholin-3-one

Guidance literature:: With sodium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In ethanol; water; benzene; at 100 ℃; for 0.5h; Microwave heating;