2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

Base Information

Chemical Name:2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline
CAS No.:76992-47-7
Molecular Formula:C₄₀H₄₁NO₅
Molecular Weight:615.769
Hs Code.:

Synonyms:2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

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Chemical Property of 2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

Chemical Property:

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Technology Process of 2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

There total 16 articles about 2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 60095-72-9
5,7-dibenzyloxyisoquinoline

: 76992-47-7
2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / benzene / 3 h / Heating

2: 1.) Mg, 1,2-dibromoethane, 2.) NaBH₄, AcOH / 1.) THF, reflux, 1 h, 2,) reflux, 1 h

With sodium tetrahydroborate; magnesium; acetic acid; ethylene dibromide; In benzene;
DOI:10.1248/cpb.29.1848

Reference yield:

: 2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)isoquinolinium bromide

: 76992-47-7
2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: With sodium borohydride acetate; In tetrahydrofuran; for 2h; Yield given; Heating;
DOI:10.1248/cpb.29.744

Reference yield:

: 1133-49-9
2,3,4-trimethoxybenzyl chloride

: 76992-47-7
2-benzyl-5,7-dibenzyloxy-1-(3,4,5-trimethoxybenzyl)-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: Multi-step reaction with 2 steps

1: Mg / tetrahydrofuran / Heating

2: sodium monoacetoxyborohydride / 2 h / Heating

With sodium borohydride acetate; magnesium; In tetrahydrofuran;