4-(3-chlorophenyl)-1,2,5,6-tetrahydropyridine-3-carbonitrile hydrochloride

Base Information

• Chemical Name: 4-(3-chlorophenyl)-1,2,5,6-tetrahydropyridine-3-carbonitrile hydrochloride
• CAS No.: 625443-83-6
• Molecular Formula: C₁₂H₁₁ClN₂*ClH
• Molecular Weight: 255.147

Synonyms:4-(3-chlorophenyl)-1,2,5,6-tetrahydropyridine-3-carbonitrile hydrochloride

Chemical Property of 4-(3-chlorophenyl)-1,2,5,6-tetrahydropyridine-3-carbonitrile hydrochloride

Chemical Property:

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Technology Process of 4-(3-chlorophenyl)-1,2,5,6-tetrahydropyridine-3-carbonitrile hydrochloride

There total 1 articles about 4-(3-chlorophenyl)-1,2,5,6-tetrahydropyridine-3-carbonitrile hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

tert-butyl 4-(3-chlorophenyl)-5-cyano-3,6-dihydropyridine-1(2H)-carboxylate (625443-82-5) → 4-(3-chlorophenyl)-1,2,5,6-tetrahydropyridine-3-carbonitrile hydrochloride (625443-83-6)

Guidance literature:

With hydrogenchloride; In dichloromethane;

Reference yield: 37.0%

4-(3-chlorophenyl)-1,2,5,6-tetrahydropyridine-3-carbonitrile hydrochloride (625443-83-6) + 1-(4-cyanophenylmethyl)-1H-imidazol-5-ylacetic acid (179026-35-8) → 4-(3-chlorophenyl)-1-{[1-(4-cyanobenzyl)-1H-imidazol-5-yl]acetyl}-1,2,5,6-tetrahydropyridine-3-carbonitrile (625443-66-5)

Guidance literature:

With trifluoroacetic acid; In water; acetonitrile;

upstream raw materials:

tert-butyl 4-(3-chlorophenyl)-5-cyano-3,6-dihydropyridine-1(2H)-carboxylate

Downstream raw materials:

4-(3-chlorophenyl)-1-{[1-(4-cyanobenzyl)-1H-imidazol-5-yl]acetyl}-1,2,5,6-tetrahydropyridine-3-carbonitrile

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