prop-2-ynyl hexan-2-ylcarbamate

Base Information

• Chemical Name: prop-2-ynyl hexan-2-ylcarbamate
• CAS No.: 1128190-17-9
• Molecular Formula: C₁₀H₁₇NO₂
• Molecular Weight: 183.25
• Mol file: 1128190-17-9.mol

Synonyms:prop-2-ynyl hexan-2-ylcarbamate

Chemical Property of prop-2-ynyl hexan-2-ylcarbamate

Chemical Property:

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Technology Process of prop-2-ynyl hexan-2-ylcarbamate

There total 1 articles about prop-2-ynyl hexan-2-ylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

n-hexan-2-one (591-78-6) + propargyl chloroformate (35718-08-2) → prop-2-ynyl hexan-2-ylcarbamate (1128190-17-9)

Guidance literature:

With triethylsilane; iron(II,III) oxide; 1,1,1,3,3,3-hexamethyl-disilazane; In toluene; at 110 ℃; for 16h; Inert atmosphere;

DOI:10.1002/adsc.200800089

upstream raw materials:

n-hexan-2-one

propargyl chloroformate