Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester

Base Information

Chemical Name:Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester
CAS No.:84525-12-2
Molecular Formula:C₁₈H₁₈O₂S
Molecular Weight:298.406
Hs Code.:

Synonyms:Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester

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Chemical Property of Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester

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Technology Process of Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester

There total 1 articles about Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 68697-43-8,74497-72-6,74497-73-7
3-methoxy-3-phenyl-2,4-dioxabicyclo<3.2.0>heptane

: 106-45-6
para-thiocresol

: 84525-12-2
Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester

Guidance literature:: for 8h; Heating;
DOI:10.1055/s-1982-30017

Reference yield: 85.0%

: 84525-12-2
Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester

: 84525-31-5
trans-2-(4-methylphenylthio)-cyclobutanol

Guidance literature:: With potassium hydroxide; In methanol; at 60 ℃; for 3.5h;
DOI:10.1055/s-1982-30017

Reference yield:

: 84525-12-2
Benzoic acid (1S,2S)-2-p-tolylsulfanyl-cyclobutyl ester

: 84525-39-3
2-(4-methylphenylsulfanyl)cyclobutanone

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / potassium hydroxide / methanol / 3.5 h / 60 °C

2: 49 percent / DMSO, oxalyl chloride / CH₂Cl₂ / 0.08 h / -60 °C

With potassium hydroxide; oxalyl dichloride; dimethyl sulfoxide; In methanol; dichloromethane;
DOI:10.1055/s-1982-30017