(2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid

Base Information

• Chemical Name: (2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid
• CAS No.: 371252-70-9
• Molecular Formula: C₇₂H₆₄N₆O₁₀
• Molecular Weight: 1173.33

Synonyms:(2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid

Chemical Property of (2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid

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Technology Process of (2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid

There total 1 articles about (2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C72H68N6O8 (371252-69-6) → (2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid (371252-70-9)

Guidance literature:

C₇₂H₆₈N₆O₈; With phthalic acid dimethyl ester; In dichloromethane; at 20 ℃;

With sodium chlorite; In dichloromethane;

DOI:10.1021/ja0166141

Reference yield:

(2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid (371252-70-9) → (2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-((S)-2-methylamino-3-phenyl-propionyl)-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid

Guidance literature:

With piperidine; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/ja0166141

Reference yield:

(2S,3aS,8aS,2'S,3'aS,8'aS)-1,1'-Bis-{(S)-2-[(9H-fluoren-9-ylmethoxycarbonyl)-methyl-amino]-3-phenyl-propionyl}-2,3,8,8a,2',3',8',8'a-octahydro-1H,1'H-[3a,3'a]bi[pyrrolo[2,3-b]indolyl]-2,2'-dicarboxylic acid (371252-70-9) → (-)-ditryptophenaline

Guidance literature:

Multi-step reaction with 2 steps

1: piperidine / tetrahydrofuran / 20 °C

2: DCC / CH₂Cl₂ / 40 °C

With piperidine; dicyclohexyl-carbodiimide; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ja0166141

upstream raw materials:

C₇₂H₆₈N₆O₈

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