3-ACETAMIDO-5-CARBOXYBENZENEBORONIC ACID 98

Base Information

• Chemical Name: 3-ACETAMIDO-5-CARBOXYBENZENEBORONIC ACID 98
• CAS No.: 108749-15-1
• Molecular Formula: C9H10BNO5
• Molecular Weight: 222.993
• Hs Code.: 2931900090
• Mol file: 108749-15-1.mol

Synonyms:3-ACETAMIDO-5-CARBOXYBENZENEBORONIC ACID 98;3-Acetamido-5-carboxybenzeneboronic acid 98%;(3-Acetamido-5-carboxy)phenylboronic acid

Chemical Property of 3-ACETAMIDO-5-CARBOXYBENZENEBORONIC ACID 98

Chemical Property:

• Melting Point: 240-243℃
• Refractive Index: 1.593
• PSA: 106.86000
• Density: 1.43 g/cm³
• LogP: -0.90400
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

3-Acetamido-5-carboxybenzeneboronic acid 98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s): Xi
• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-ACETAMIDO-5-CARBOXYBENZENEBORONIC ACID 98

There total 1 articles about 3-ACETAMIDO-5-CARBOXYBENZENEBORONIC ACID 98 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3-(dihydroxyboryl)-5-acetamidobenzoate (1071959-03-9) → 3-(dihydroxyboryl)-5-acetamidobenzoic acid (108749-15-1)

Guidance literature:

With lithium hydroxide monohydrate; water; In tetrahydrofuran; at 20 ℃;

DOI:10.1021/jm9009718

Reference yield: 35.0%

N-(3-bromo-1-naphthyl)-2,3,5,6-tetramethyl-benzenesulfonamide + 3-(dihydroxyboryl)-5-acetamidobenzoic acid (108749-15-1) → 3-acetamido-5-[4-[(2,3,5,6-tetramethylphenyl)sulfonylamino]-2-naphthyl]benzoic acid

Guidance literature:

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; sodium carbonate; In 1,4-dioxane; at 90 ℃; for 5h;

upstream raw materials:

methyl 3-(dihydroxyboryl)-5-acetamidobenzoate

Refernces