N-(2-mercaptophenyl)-N-methylacetamide

Base Information

• Chemical Name: N-(2-mercaptophenyl)-N-methylacetamide
• CAS No.: 50498-76-5
• Molecular Formula: C₉H₁₁NOS
• Molecular Weight: 181.258
• Mol file: 50498-76-5.mol

Synonyms:N-(2-mercaptophenyl)-N-methylacetamide

Chemical Property of N-(2-mercaptophenyl)-N-methylacetamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of N-(2-mercaptophenyl)-N-methylacetamide

There total 2 articles about N-(2-mercaptophenyl)-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N-{2-[2-(acetylmethylamino)phenyldisulfanyl]phenyl}-N-methylacetamide (58177-11-0) → N-(2-mercaptophenyl)-N-methylacetamide (50498-76-5)

Guidance literature:

With sodium tetrahydroborate; In tetrahydrofuran; ethanol; at 20 ℃; for 4h;

DOI:10.1039/b714386a

Reference yield:

→ N-(2-mercaptophenyl)-N-methylacetamide (50498-76-5)

Guidance literature:

Na-o-(acetyl-methylamino)-thiophenolat, H⁺;

Reference yield: 18.0%

{hydrotris(3,5-dimethyl-1-pyrazolyl)borate}dioxomolybdenum(VI)Cl + N-(2-mercaptophenyl)-N-methylacetamide (50498-76-5) → Tp*MoO2(S-o-MeCONMeC6H4)

Guidance literature:

With triethylamine; In dichloromethane; (under Ar, Schlenk); mixt. of ligand and N(CH2CH3)3 in CH2Cl2 added to suspn. of Mo-complex in CH2Cl2 at room temp., stirred overnight; solvent removed under reduced pressure, chromd. on silica gel with MeCN-toluene (1:4), collected, solvent evapd.;

DOI:10.1039/b714386a

upstream raw materials:

N-{2-[2-(acetylmethylamino)phenyldisulfanyl]phenyl}-N-methylacetamide