1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione

Base Information

Chemical Name:1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione
CAS No.:1030601-57-0
Molecular Formula:C₃₈H₅₈O₈Si₂
Molecular Weight:699.045
Hs Code.:

Synonyms:1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione

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Chemical Property of 1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione

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Technology Process of 1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione

There total 1 articles about 1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1030601-62-7
C₃₈H₅₈O₈Si₂

: 1030601-57-0
1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione

Guidance literature:: With sodium hydride; In tetrahydrofuran; for 1.5h; Inert atmosphere; Reflux;
DOI:10.1021/ol800665w

Reference yield: 60.0%

: 1030601-57-0
1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione

: 1030601-58-1
7-O-tert-butyldimethylsilyl-4'-O-pivaloylcannflavin B

: 1030601-60-5
C₃₂H₄₂O₇Si

Guidance literature:: 1-[2,4-bis(tert-butyldimethylsilyloxy)-6-hydroxy-3-prenylphenyl]-3-(4-pivaloyloxy-3-methoxyphenyl)-1,3-propanedione; With chloro-trimethyl-silane; copper dichloride; In acetonitrile; at 20 ℃; for 1.5h; Inert atmosphere;

With water; In acetonitrile; regioselective reaction;
DOI:10.1021/ol800665w