1-bromo-3,5-diallylbenzene

Base Information

Chemical Name:1-bromo-3,5-diallylbenzene
CAS No.:1442416-61-6
Molecular Formula:C₁₂H₁₃Br
Molecular Weight:237.139
Hs Code.:

Synonyms:1-bromo-3,5-diallylbenzene

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Chemical Property of 1-bromo-3,5-diallylbenzene

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Technology Process of 1-bromo-3,5-diallylbenzene

There total 2 articles about 1-bromo-3,5-diallylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 262300-30-1
1-allyl-3,5-dibromobenzene

: 106-95-6
allyl bromide

: 1442416-61-6
1-bromo-3,5-diallylbenzene

Guidance literature:: 1-allyl-3,5-dibromobenzene; With n-butyllithium; isopropylmagnesium chloride; In tetrahydrofuran; hexane; at -5 ℃; for 8.5h; Inert atmosphere;

allyl bromide; With copper(l) cyanide; In tetrahydrofuran; hexane; at -5 - 20 ℃; for 15.5h; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.130

Reference yield:

: 626-39-1
1,3,5-trisbromobenzene

: 1442416-61-6
1-bromo-3,5-diallylbenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: isopropylmagnesium chloride; n-butyllithium / tetrahydrofuran; hexane / 8.5 h / -5 °C / Inert atmosphere

1.2: 15.5 h / -5 - 20 °C / Inert atmosphere

2.1: isopropylmagnesium chloride; n-butyllithium / tetrahydrofuran; hexane / 8.5 h / -5 °C / Inert atmosphere

2.2: 15.5 h / -5 - 20 °C / Inert atmosphere

With n-butyllithium; isopropylmagnesium chloride; In tetrahydrofuran; hexane;
DOI:10.1016/j.tet.2013.04.130

Reference yield: 77.0%

: 1442416-61-6
1-bromo-3,5-diallylbenzene

: 1442416-62-7
1,3-diallyl-5-iodobenzene

Guidance literature:: 1-bromo-3,5-diallylbenzene; With n-butyllithium; isopropylmagnesium chloride; In tetrahydrofuran; hexane; at -5 ℃; for 6.5h; Inert atmosphere;

With iodine; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 18h; Inert atmosphere;
DOI:10.1016/j.tet.2013.04.130