(S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid

Base Information

Chemical Name:(S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid
CAS No.:1353054-42-8
Molecular Formula:C₃₃H₄₆N₂O₆
Molecular Weight:566.738
Hs Code.:

Synonyms:(S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid

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Chemical Property of (S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid

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Technology Process of (S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid

There total 1 articles about (S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 76387-70-7
(S)-3-amino-2-tert-butoxycarbonylaminopropionic acid

: 147299-36-3
6-<4-(4-n-hexylbenzoyl)phenyl>hexanoic acid

: 1353054-42-8
(S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid

Guidance literature:: 6-<4-(4-n-hexylbenzoyl)phenyl>hexanoic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.166667h;

(S)-3-amino-2-tert-butoxycarbonylaminopropionic acid; In methanol; dichloromethane; at 20 ℃; for 12h; Darkness;
DOI:10.1016/j.bmc.2011.10.043

Reference yield: 78.0%

: 143-27-1
hexadecylamine

: 1353054-42-8
(S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid

: 1353054-43-9
(S)-tert-butyl 1-(hexadecylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)-1-oxopropan-2-ylcarbamate

Guidance literature:: (S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid; With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 0.166667h;

hexadecylamine; In dichloromethane; at 20 ℃; for 6h; Darkness;
DOI:10.1016/j.bmc.2011.10.043

Reference yield:

: 1353054-42-8
(S)-2-(tert-butoxycarbonylamino)-3-(6-(4-(4-hexylbenzoyl)phenyl)hexanamido)propanoic acid

: 1353054-44-0
(S)-N-(2-amino-3-(hexadecylamino)-3-oxopropyl)-6-(4-(4-hexylbenzoyl)phenyl)hexanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.17 h

1.2: 6 h / 20 °C / Darkness

2.1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C / Darkness

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In dichloromethane;
DOI:10.1016/j.bmc.2011.10.043