4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile

Base Information

• Chemical Name: 4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile
• CAS No.: 1414268-69-1
• Molecular Formula: C₂₅H₁₅ClN₂O₄
• Molecular Weight: 442.858

Synonyms:4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile

Chemical Property of 4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile

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Technology Process of 4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile

There total 1 articles about 4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.04%

4,5-dichlorophthalonitrile (139152-08-2) + 7-hydroxy-4-(4-methoxyphenyl)-8-methyl-2H-2-chromenone (370583-62-3) → 4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile (1414268-69-1) + 4,5-bis(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile (1414268-72-6)

Guidance literature:

4,5-dichlorophthalonitrile; 7-hydroxy-4-(4-methoxyphenyl)-8-methyl-2H-2-chromenone; In N,N-dimethyl-formamide; for 0.166667h; Inert atmosphere;

With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 240h; Inert atmosphere;

DOI:10.1016/j.poly.2012.08.080

Reference yield: 55.46%

4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile (1414268-69-1) + 4,5-bis(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile (1414268-72-6) + zinc(II) acetate dihydrate (5970-45-6) → 2,3,9,10,16,17,23,24-octakis(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalocyaninato zinc(II)

Guidance literature:

In N,N-dimethyl-formamide; at 320 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1016/j.poly.2012.08.080

Reference yield: 38.1%

4-chloro-5-(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile (1414268-69-1) + 4,5-bis(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalonitrile (1414268-72-6) + cobalt(II) diacetate tetrahydrate (6147-53-1) → 2,3,9,10,16,17,23,24-octakis(4-(4-methoxyphenyl)-8-methylcoumarin-7-yloxy)phthalocyaninato cobalt(II)

Guidance literature:

In N,N-dimethyl-formamide; at 320 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1016/j.poly.2012.08.080

upstream raw materials:

4,5-dichlorophthalonitrile

7-hydroxy-4-(4-methoxyphenyl)-8-methyl-2H-2-chromenone

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