C₁₀H₁₉ClO₃

Base Information

Chemical Name:C₁₀H₁₉ClO₃
CAS No.:1293966-42-3
Molecular Formula:C₁₀H₁₉ClO₃
Molecular Weight:222.712
Hs Code.:

C<sub>10</sub>H<sub>19</sub>ClO<sub>3</sub>

Synonyms:C₁₀H₁₉ClO₃

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Chemical Property of C₁₀H₁₉ClO₃

Chemical Property:

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Technology Process of C₁₀H₁₉ClO₃

There total 1 articles about C₁₀H₁₉ClO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: C₂₀H₂₆ClNO₅

: 1293966-42-3
C₁₀H₁₉ClO₃

: C₁₀H₁₉ClO₃

: 40217-17-2,90719-32-7,120574-96-1,102029-44-7
(R)-4-(phenylmethyl)-2-oxazolidinone

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water; at 20 ℃; for 20.5h;
DOI:10.1021/acs.orglett.9b00722

Reference yield:

: 1293966-42-3
C₁₀H₁₉ClO₃

: C₆₃H₁₀₇ClO₁₃Si₂

Guidance literature:: Multi-step reaction with 13 steps

1.1: Dess-Martin periodane / dichloromethane / 3 h / Inert atmosphere

2.1: toluene / 16 h / -78 °C / Molecular sieve; Inert atmosphere

3.1: dmap; triethylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: ozone; triphenylphosphine / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: tert.-butyl lithium / diethyl ether; pentane / 0.5 h / -78 °C / Inert atmosphere

5.2: 2 h / -78 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / acetone / 12 h / 20 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

8.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

9.1: tert.-butyl lithium / diethyl ether; pentane / 0.5 h / -78 °C / Inert atmosphere

9.2: 2 h / -78 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

11.1: dmap; camphor-10-sulfonic acid; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 30 °C

12.1: 1H-imidazole; dmap / dichloromethane / 15 h / 40 °C / Inert atmosphere

13.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 18 h / Inert atmosphere; Reflux

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; dmap; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; iodine; tert.-butyl lithium; pyridinium p-toluenesulfonate; Dess-Martin periodane; ozone; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; toluene; pentane; 1.1: Dess-Martin oxidation;
DOI:10.1021/ol2007296

Reference yield:

: 1293966-42-3
C₁₀H₁₉ClO₃

: 1293966-80-9
C₅₉H₉₇ClO₁₃Si

Guidance literature:: Multi-step reaction with 11 steps

1.1: Dess-Martin periodane / dichloromethane / 3 h / Inert atmosphere

2.1: toluene / 16 h / -78 °C / Molecular sieve; Inert atmosphere

3.1: dmap; triethylamine / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

4.1: ozone; triphenylphosphine / dichloromethane / -78 - 20 °C / Inert atmosphere

5.1: tert.-butyl lithium / diethyl ether; pentane / 0.5 h / -78 °C / Inert atmosphere

5.2: 2 h / -78 °C / Inert atmosphere

6.1: pyridinium p-toluenesulfonate / acetone / 12 h / 20 °C / Inert atmosphere

7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

8.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 3 h / 0 °C / Inert atmosphere

9.1: tert.-butyl lithium / diethyl ether; pentane / 0.5 h / -78 °C / Inert atmosphere

9.2: 2 h / -78 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

11.1: dmap; camphor-10-sulfonic acid; dicyclohexyl-carbodiimide / dichloromethane / 15 h / 30 °C

With 1H-imidazole; dmap; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; iodine; tert.-butyl lithium; pyridinium p-toluenesulfonate; Dess-Martin periodane; ozone; triethylamine; dicyclohexyl-carbodiimide; triphenylphosphine; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; toluene; pentane; 1.1: Dess-Martin oxidation;
DOI:10.1021/ol2007296