(3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

Base Information

Chemical Name:(3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester
CAS No.:155989-61-0
Molecular Formula:C₁₅H₂₆N₂O₄Si
Molecular Weight:326.468
Hs Code.:

Synonyms:(3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

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Chemical Property of (3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

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Technology Process of (3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

There total 10 articles about (3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 138770-70-4
[3-(Benzyloxycarbonyl-methyl-amino)-4,5-dimethoxy-phenyl]-carbamic acid 2-trimethylsilanyl-ethyl ester

: 155989-61-0
(3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethanol; for 2h; Ambient temperature;
DOI:10.1016/S0040-4020(01)85065-1

Reference yield:

: 2916-68-9
2-(Trimethylsilyl)ethanol

: 155989-61-0
(3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 2 h / 60 °C

2: 100 percent / hydrogen / 10percent Pd-C / ethanol / 2 h / Ambient temperature

With hydrogen; palladium on activated charcoal; In ethanol; toluene;
DOI:10.1016/S0040-4020(01)85065-1

Reference yield:

: 22027-96-9
5-nitroveratral

: 155989-61-0
(3,4-Dimethoxy-5-methylamino-phenyl)-carbamic acid 2-trimethylsilanyl-ethyl ester

Guidance literature:: Multi-step reaction with 9 steps

1: iron dust, 12 M HCl / methanol / 10 h / Heating

2: Na₂CO₃ / diethyl ether; H₂O / 1.) 0 deg C, 30 min; 2.) room temp., 2 h

3: 77 percent / NaH / dimethylformamide / 3 h / Ambient temperature

4: 89 percent / Jones reagent / acetone / 2 h / Ambient temperature

5: tetrahydrofuran / 2 h / Ambient temperature

6: 5 M aq. NaN₃ / H₂O / 2 h / Ambient temperature

7: toluene / 1 h / Heating

8: toluene / 2 h / 60 °C

9: 100 percent / hydrogen / 10percent Pd-C / ethanol / 2 h / Ambient temperature

With hydrogenchloride; sodium azide; jones reagent; hydrogen; iron; sodium hydride; sodium carbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; N,N-dimethyl-formamide; acetone; toluene;
DOI:10.1016/S0040-4020(01)85065-1