Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester

Base Information

Chemical Name:Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester
CAS No.:853929-35-8
Molecular Formula:C₂₃H₂₆O₅
Molecular Weight:382.456
Hs Code.:

Synonyms:Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester

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Chemical Property of Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester

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Technology Process of Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester

There total 6 articles about Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 853929-33-6
Benzoic acid (S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-ynyl ester

: 853929-35-8
Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester

Guidance literature:: With hydrogen; Lindlar catalyst; In hexane; at 20 ℃;
DOI:10.1016/j.tetlet.2005.03.175

Reference yield:

: 853929-30-3
Benzoic acid (S)-1-benzyloxymethyl-7-hydroxy-hept-3-ynyl ester

: 853929-35-8
Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: Jones reagent / acetone / 0 °C

1.2: 93 percent / TMSCl; 2,2-dimethoxypropane / 20 °C

2.1: 98 percent / H₂ / Lindlar cat. / hexane / 20 °C

With jones reagent; hydrogen; Lindlar catalyst; In hexane; acetone; 1.1: Jones oxidation;
DOI:10.1016/j.tetlet.2005.03.175

Reference yield:

: 853929-20-1
(2S)-1-(benzyloxy)-8-((tetrahydro-2H-pyran-2-yl)oxy)oct-4-yn-2-ol

: 853929-35-8
Benzoic acid (Z)-(S)-1-benzyloxymethyl-6-methoxycarbonyl-hex-3-enyl ester

Guidance literature:: Multi-step reaction with 4 steps

1.1: 92 percent / pyridine / 0 - 20 °C

2.1: 88 percent / pyridinium p-toluenesulfonate / methanol / 20 °C

3.1: Jones reagent / acetone / 0 °C

3.2: 93 percent / TMSCl; 2,2-dimethoxypropane / 20 °C

4.1: 98 percent / H₂ / Lindlar cat. / hexane / 20 °C

With pyridine; jones reagent; hydrogen; pyridinium p-toluenesulfonate; Lindlar catalyst; In methanol; hexane; acetone; 3.1: Jones oxidation;
DOI:10.1016/j.tetlet.2005.03.175