N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane

Base Information

Chemical Name:N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane
CAS No.:603957-80-8
Molecular Formula:C₂₅H₂₈N₄O₅
Molecular Weight:464.521
Hs Code.:

Synonyms:N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane

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Chemical Property of N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane

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Technology Process of N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane

There total 5 articles about N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: N,N'-bis(salicylidene)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane

: 603957-80-8
N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane

Guidance literature:: With sodium tetrahydroborate; In methanol; at 60 ℃; for 2h;
DOI:10.1039/b300621m

Reference yield:

: 63-91-2,25191-15-5,658-69-5,67675-33-6
L-phenylalanine

: 603957-80-8
N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane

Guidance literature:: Multi-step reaction with 5 steps

1: HNO₃ / H₂SO₄ / 1 h / 0 - 5 °C

2: 88.3 percent / HCl / methanol / 5 h / 20 °C

3: 70 percent / 24 h / 20 °C

4: 88 percent / methanol / 18 h / 40 °C

5: 90 percent / NaBH₄ / methanol / 2 h / 60 °C

With hydrogenchloride; sodium tetrahydroborate; nitric acid; In methanol; sulfuric acid;
DOI:10.1039/b300621m

Reference yield:

: 949-99-5
4-nitro-3-phenyl-L-alanine

: 603957-80-8
N,N'-bis(2-hydroxybenzyl)-2-(p-nitrobenzyl)-3-monooxo-1,4,7-triazaheptane

Guidance literature:: Multi-step reaction with 4 steps

1: 88.3 percent / HCl / methanol / 5 h / 20 °C

2: 70 percent / 24 h / 20 °C

3: 88 percent / methanol / 18 h / 40 °C

4: 90 percent / NaBH₄ / methanol / 2 h / 60 °C

With hydrogenchloride; sodium tetrahydroborate; In methanol;
DOI:10.1039/b300621m